Award Abstract # 1625422
MRI: Acquisition of a next-generation electron microprobe at the University of Minnesota

NSF Org: EAR
Division Of Earth Sciences
Recipient: REGENTS OF THE UNIVERSITY OF MINNESOTA
Initial Amendment Date: August 12, 2016
Latest Amendment Date: August 12, 2016
Award Number: 1625422
Award Instrument: Standard Grant
Program Manager: Russell Kelz
EAR
 Division Of Earth Sciences
GEO
 Directorate for Geosciences
Start Date: August 15, 2016
End Date: January 31, 2019 (Estimated)
Total Intended Award Amount: $1,192,105.00
Total Awarded Amount to Date: $1,192,105.00
Funds Obligated to Date: FY 2016 = $1,192,105.00
History of Investigator:
  • Marc Hirschmann (Principal Investigator)
    mmh@umn.edu
  • David Kohlstedt (Co-Principal Investigator)
  • Donna Whitney (Co-Principal Investigator)
  • Jake Bailey (Co-Principal Investigator)
  • Anette von der Handt (Co-Principal Investigator)
Recipient Sponsored Research Office: University of Minnesota-Twin Cities
2221 UNIVERSITY AVE SE STE 100
MINNEAPOLIS
MN  US  55414-3074
(612)624-5599
Sponsor Congressional District: 05
Primary Place of Performance: University of Minnesota-Twin Cities
Tate Hall 116 Church St SE
Minneapolis
MN  US  55455-2070
Primary Place of Performance
Congressional District:
05
Unique Entity Identifier (UEI): KABJZBBJ4B54
Parent UEI:
NSF Program(s): Major Research Instrumentation
Primary Program Source: 01001617DB NSF RESEARCH & RELATED ACTIVIT
Program Reference Code(s):
Program Element Code(s): 118900
Award Agency Code: 4900
Fund Agency Code: 4900
Assistance Listing Number(s): 47.050

ABSTRACT

The project is for the University of Minnesota to acquire a next-generation electron microprobe to replace a well-used but aging 23-year-old instrument. This investment provides the newest capabilities in high-resolution mapping of elements in rocks, organic material, and high-technology materials. This support is congruent with NSFs mission of promoting the progress of science and advancing the national health, prosperity and welfare, given the importance of expanding the frontiers of knowledge in the earth and environmental sciences, engineering, archeology, biotechnology and dentistry. The new instrument serves a national research community as well as universities in Minnesota, western Wisconsin, the Dakotas, and Montana.

The University of Minnesota will acquire a next-generation electron microprobe, which houses multiple energy-dispersive spectrometers, including a Soft X-ray Emission Spectrometer (SXES). The instrument means that elements can be mapped at a high-spatial resolution of 200 nanometers. The SXES provides for a new capability in the analysis of light elements and organic matter, phosphates, carbonates, and polymers. Research programs at Minnesota that depend on electron microprobe analyses include experimental petrology, mineral and rock physics, geobiology, geomicrobiology, and bioremediation, tectonics and metamorphic petrology, mineral and rock magnetism, aqueous geochemistry, paleoclimate, and economic geology.

PUBLICATIONS PRODUCED AS A RESULT OF THIS RESEARCH

Note:  When clicking on a Digital Object Identifier (DOI) number, you will be taken to an external site maintained by the publisher. Some full text articles may not yet be available without a charge during the embargo (administrative interval).

Some links on this page may take you to non-federal websites. Their policies may differ from this site.

Aurélien Moy, John Fournelle and Anette von der Handt. "Quantitative measurement of iron-silicides by EPMA using the Fe L? and L? X-ray lines: a new twist to an old approach." Microscopy & Microanalysis , 2019 https://doi.org/10.1017/S1431927619000436
Aurélien Moy, John Fournelle and Anette von der Handt. "Solving the Iron Quantification Problem in Low kV EPMA: An essential step toward improved analytical spatial resolution in electron probe microanalysis. I. Olivines" American Mineralogist , 2019 10.2138/am-2019-6865
Liu, L., Sun, C., Zhang, C., Voyles, P.M., Fournelle, J., von der Handt, A. and Perepezko, J.H. "Examination of B in the Mo solid solution (Moss) in Moss+ Mo5SiB2+ Mo2B alloys" Scripta Materialia , v.163 , 2019 , p.62 https://doi.org/10.1016/j.scriptamat.2019.01.003

PROJECT OUTCOMES REPORT

Disclaimer

This Project Outcomes Report for the General Public is displayed verbatim as submitted by the Principal Investigator (PI) for this award. Any opinions, findings, and conclusions or recommendations expressed in this Report are those of the PI and do not necessarily reflect the views of the National Science Foundation; NSF has not approved or endorsed its content.

This award facilitated the purchase of a state-of-the-art Electron Probe Microanalyzer (EPMA), which combines scanning electron microscope imaging to characterize textures of materials at very high spatial resolution (30 nanometers) with the capability to determine their composition in the sub-micrometer range.   The EPMA is used chiefly for Earth sciences research.   Topics that are addressed include the formation and evolution of terrestrial planets (Earth, Moon, Mars), the origins of volcanos and mountain ranges, geomagnetism, the origin of economic mineral deposits, and interactions between rocks and microbial life.  The EPMA is also used in other academic physical science and engineering research, including physics, chemistry, biology, material sciences, chemical engineering, civil engineering, aeronautical engineering, and dentistry.  Additional users come from government and industrial organizations interested in topics that range from minerals exploration, remediation of mine waste and ground water contamination, and development of new biomedical devices.  

The new EPMA improves greatly on previous similar instruments.  The 3rd generation field emission electron microprobe allows highly improved spatial resolution (see figures).  The new generation of spectrometers allows quantitative analysis of elements in concentrations as low as 10 parts per million and characterization of chemical bonding between elements in compounds through the novel soft X-ray spectrometer (SXES).  It also facilitates creation of high spatial resolution (less than 1 micrometer) maps that show variations in chemical concentrations and chemical bonding.

 The new EPMA is used for routine analyses of natural and engineered materials, but is also used for development of novel analytical methods and tools that facilitate new applications of EPMA instruments, and these are adopted in other laboratories around the world. 

The new instrument is also used for teaching and education of graduate and undergraduate students, for training of junior and senior scientists in electron microscopy and quantitative microanalysis techniques, and in outreach activities that reach the general public through museum exhibits as well as in electronic and print media.

 

 


Last Modified: 07/11/2019
Modified by: Marc M Hirschmann

Please report errors in award information by writing to: awardsearch@nsf.gov.

Print this page

Back to Top of page