Award Abstract # 1562960
Collaborative Research: Modeling Material Microstructure Evolution and Fatigue Life of High Strength Metal Components Produced by Laser Melting Additive Process

NSF Org: CMMI
Division of Civil, Mechanical, and Manufacturing Innovation
Recipient: PURDUE UNIVERSITY
Initial Amendment Date: March 2, 2016
Latest Amendment Date: March 2, 2016
Award Number: 1562960
Award Instrument: Standard Grant
Program Manager: Khershed Cooper
khcooper@nsf.gov
 (703)292-7017
CMMI
 Division of Civil, Mechanical, and Manufacturing Innovation
ENG
 Directorate for Engineering
Start Date: April 1, 2016
End Date: March 31, 2020 (Estimated)
Total Intended Award Amount: $150,000.00
Total Awarded Amount to Date: $150,000.00
Funds Obligated to Date: FY 2016 = $150,000.00
History of Investigator:
  • C. Richard Liu (Principal Investigator)
Recipient Sponsored Research Office: Purdue University
2550 NORTHWESTERN AVE # 1100
WEST LAFAYETTE
IN  US  47906-1332
(765)494-1055
Sponsor Congressional District: 04
Primary Place of Performance: Purdue University
315 North Grant Street
West Lafayette
IN  US  47907-2023
Primary Place of Performance
Congressional District:
04
Unique Entity Identifier (UEI): YRXVL4JYCEF5
Parent UEI: YRXVL4JYCEF5
NSF Program(s): Manufacturing Machines & Equip
Primary Program Source: 01001617DB NSF RESEARCH & RELATED ACTIVIT
Program Reference Code(s): 082E, 083E, 9146, MANU
Program Element Code(s): 146800
Award Agency Code: 4900
Fund Agency Code: 4900
Assistance Listing Number(s): 47.041

ABSTRACT

Additive manufacturing can enable industry to produce on-demand parts at a remote site, in space, or in a battlefield, with minimal inventory, delivery time, and tooling cost. It can also enable researchers to explore new material compositions leading to customized novel properties. To ensure quality of components in laser melting (one of the additive manufacturing processes) and reduce the lead time, it is critical to be able to evaluate material microstructure changes in response to the dynamic high thermal gradient in the process, and the strength of constructed materials under static and dynamic loads after the process. This award supports fundamental research to enable modeling and simulation methods that allow for realistic predictions, process design and optimization, and equipment design of laser melting additive process. The obtained knowledge provides the foundation for researchers and manufacturers to engineer new materials in small lot size at low cost by using laser melting additive process. It can also contribute to understanding the behavior of a broad range of materials in laser melting. Research results will enhance current engineering courses, and provide cross-disciplinary training opportunities for graduate students.

The research objectives are to: (1) acquire knowledge on the mechanism of non-equilibrium solidification in laser melting, (2) determine the effects of non-uniform cyclic thermal history due to multilayer construction on microstructure changes, and (3) establish the relationship between the microstructure resulted from laser melting and the material performances. To achieve the first objective, a thermo-mechanical finite element analysis will be constructed to simulate the material addition process of laser melting, a phase-field approach will be created to calculate the time-dependent growth of alloy phase field based on the computed thermal history, and single-pass and multilayer laser melting experiments will be conducted on a medium carbon steel. The correlation between high thermal gradients from computation and the solute trapping phenomenon from experimental observation will be made to reveal the non-equilibrium solidification mechanism. To achieve the second objective, the microstructure evolutions under both single pass and multilayer laser melting processes are compared using the phase field approach, and verified by experiments. Microstructure variations in terms of grain size, phase composition and distribution will be obtained, resulting from different thermal histories of material points. To achieve the third objective, the analytical models for estimating strengths will be established based on the obtained material microstructure, and the fatigue crack initiation life will be estimated based on the minimum energy principle applied when a crack is created along the weakest material point and path.

PUBLICATIONS PRODUCED AS A RESULT OF THIS RESEARCH

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Cheng Peng, C. Richard Liu, *, Rohit Voothaluru, Chun-Yu Ou, Zhikun Liu "An Exploratory Investigation of the Mechanical Properties of the Nanostructured Porous Materials Deposited by Laser-induced Chemical Solution Synthesis" Transaction of the ASME, Journal of Micro and Nano-Manufacturing , v.Vol 5 , 2017 ISSN 2166-0468
Chun-Yu Ou, and C. Richard Liu "The effects of grain size and strain amplitude on persistent slip band formation and fatigue crack initiation. August 22, 2019." Metallurgical and Materials Transactions A, , v.August , 2019 https://doi.org/10.1007/s11661-019-05423-6.
Chun-Yu Ou, Rohit Voothaluru, and C. Richard Liu "A methodology for incorporating the effect of grain size on the energy efficiency coefficient for fatigue crack initiation estimation in polycrystalline metal." Journal of Metals , v.10 , 2020 , p.355 https://doi.org/10.3390/met10030355.
Siyu Liu, Chun-Yu Ou, and C. Richard Liu "Temporal and spatial temperature modelling for understanding pulsed laser induced solution based nanomanufacturing" Nanotechnology , v.31 , 2020 https://doi.org/10.1088/1361-6528/ab8c09

PROJECT OUTCOMES REPORT

Disclaimer

This Project Outcomes Report for the General Public is displayed verbatim as submitted by the Principal Investigator (PI) for this award. Any opinions, findings, and conclusions or recommendations expressed in this Report are those of the PI and do not necessarily reflect the views of the National Science Foundation; NSF has not approved or endorsed its content.

Economic production of small lots of components is a long-standing problem in industry. A potential solution is additive manufacturing (AM) which has low preparation cost and high capability for producing complex geometry. It is a manufacturing process that adds material bottom-up. Non-critical components fabricated via AM are now being used in motor vehicles, consumer products, medical products and aerospace devices. 

For engineering applications, high value-added components require consistency in fatigue properties. However, components fabricated by AM have large variation in the fatigue properties compared to those by conventional manufacturing processes. To alleviate unpredictable catastrophic failures, it is essential to study fatigue behavior. Previous study reported that fatigue crack initiation mechanism accounts for a large portion of fatigue life, especially for low amplitude and high cycle fatigue under real world loading conditions. However, this major portion of fatigue life prediction is mostly ignored by main-stream researchers working on fatigue modeling. This research has made a major advance in this new fatigue research and modeling direction. 

The objective of this research is to develop a fatigue crack initiation model for metal components produced by AM. To improve life prediction accuracy, the model must incorporate the effect of different microstructures produced in the components, which is complex due to numerous cycles of re-heating and re-cooling processes. The project is thus separated into three tasks: (1) developing a temperature model to account for the thermal cycling history, (2) modeling the component’s microstructures produced by the cycling temperatures for the potential crack initiation zone, and (3) developing a fatigue crack initiation model for life estimation. A summary of each task is provided in the following.

First, the role of temperature model is to predict the temperature history at each material point for the material volume of interest, as an input to the microstructure-temperature model for predicting the distribution of microstructures resulted from the AM process. The existing temperature models are computationally expensive to for accurate prediction of the temperature resulted from repetitive heating and cooling. The main reason is that these models considered entire boundary conditions of all the material points. In this project, we proposed and employed the new concept of effective computation zone, which can save the computational time significantly for the AM process. 

Second, The microstructures considered consists the grain size and the phase. The grain size variation is modeled by using representative volume element, which is defined as a volume of heterogeneous material that is sufficiently large to be statistically representative of the real component’s microstructure. The material phase of each point is obtained by modeling the process of phase transformation. A continuous cooling transformation (CCT) diagram is used with a thermal model for predicting the resultant microstructure phases. Since traditional CCT diagrams are developed based on slow and monotonic cooling processes, such as furnace cooling and air cooling, which are very different from the repetitive heating and cooling processes in AM. In this study, a new general methodology is presented to create CCT diagrams for materials fabricated by AM. The result showed that the effect of the segmented duration within the critical temperature range, which induced precipitate formation, could be cumulative.

Third, the existing fatigue crack initiation life model has poor accuracy. One reason for the poor accuracy is the coefficients change due to the variation in the microstructure is not accounted for. In this research task, a semi-empirical fatigue crack initiation model was developed with microstructure-dependent coefficients of maximum persistent slipband width, energy efficiency coefficient, resolved shear stress and plastic slip rate per cycle. Methods of determining these coefficients as functions of microstructures, which can improve the accuracy of fatigue life estimation. 

The outcome of this project is to provide a new engineering tool for understanding and designing the melting AM process for metals based on scientific models. With this tool, the fundamental mechanism contributing to a large variation of the fatigue life of the metal components made by AM process can be understood, attributed, and predicted. The seemly ‘stochastic’ nature of fatigue life of the AM components can be changed to be more deterministic and pedictable. This approach represents a major advance in new and effective fatigue modeling and microstructure prediction methodology for AM made components.  The models and methodology developed can be used as tools for research, design, and control for laser-based AM process applications.

 

 


Last Modified: 06/25/2020
Modified by: C. Richard Liu

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